Section for Functional Oxides DTU Energy Technical University of Denmark Oliver Liebe PhD Student in Physics Fysikvej, Building 310, 2800 Kgs. Lyngby Cover picture
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Internship at the Deutsches Elektronen-Synchrotron, 2022




For a two-month period in the summer of 2022, I lived on-site at the Deutsches Elektronen-Synchrotron (DESY) in Hamburg, Germany for the re-opening year of the summer school programme following the COVID-19 pandemic.

The programme consisted of approximately 65 students from around the world, divided into two major sub-groups: The High Energy Physics (HEP) group and the Photon Science group, to the latter of which I belonged. During my time at DESY, I attented lectures on a variety of topics, including the basics of synchrotron radiation, the use of X-ray in matter characterisation, and light characterisation totalling around 36 hours of lectures.
I also had the opportunity to utilise the PETRA III synchrotron for X-ray characterisation, visit the FLASH free-electron laser, and the European XFEL. A link to the various facilities at DESY can be found on the DESY website.

Besides the lectures and facility visits, the majority of my time was spent working on a project supervised by Mr. Constantin Harder and Dr. Stephan Roth. The project was based on the coating of porous materials The work produced during this time can be found here: "Functional Cellulose Ligning Coating on Porous Materials" and below you will find a brief summary of the work carried out during this time.

Introduction


Cellulose-nano-fibrils (CNFs) and lignins are present in the cell walls of plants and are known to be biodegradable and renewable materials. They are environmentally friendly, have an excellent bio-compatibility, and are of low toxicity1. The combination of these materials has been shown to have a high potential for use in the coating of porous materials2,3. They are complimentary materials due to the bio-polymeric properties of CNFs to act as a platform, onto which the UV-absorbing properties of lignin4 can be added.

The general procedure in the work is as follows:
  1. Preparation of the CNF solution
  2. Preparation of the lignin solution
  3. Coating of the porous material
  4. Characterisation of the coated material


References


[1] S. S. Jaffar, S. Saallah, M. Misson, S. Siddiquee, J. Roslan, S. Saalah, and W. Lenggoro. Recent Developments and Environmental Application of Nanocellulose-Based Membranes. Membranes, 287,. 2022.
[2] A. H. Tayeb, M. Tajvidi, and D. Bousfield. Paper-Based Oil Barrier Packaging using Lignin-Containing Cellulose Nanofibrils. Molecules, 25, 2020.
[3] Y. Zhong, L. Gu, S. Wang, Y. Jin, and H. Xiao. Green and Hydrophobic Coatings based on Tailor-modified Lignocellulose Nanofibrils for Self-Cleaning Purposes. Ind. Eng. Chem. Res, 58, 2019.
[4] H. Sadeghifar and A. Ragauskas. Lignin as a UV light Blocker - A Review. Polymer, 12, 2020.